Synthesis and growth mechanism of whisker-like Mg2B2O5 crystals by an easy and environmentally hospitable non-aqueous ionic liquid method


An environmentally hospitable NaCl non-aqueous ionic liquid methodology has been utilized to arrange single crystalline whisker-like Mg2B2O5 crystals, that were synthesised by annealing a ground mixture of H3BO3, MgCl2·6H2O, NaCl and surfactant nonylphenyl ether (9) at 850°C for two h. The systemically comparative experiments are performed to perceive the formation mechanism of whisker-like Mg2B2O5 crystals. The results demonstrated that each non-aqueous ionic liquid and nonylphenyl ether (nine) played vital roles within the formation of whisker-like Mg2B2O5 crystals. Primarily based on the experimental results and analysis, a reasonable growth mechanism of whisker-like Mg2B2O5 crystals is proposed. This reported work exposes a relative low-temperature strategy for the synthesis of single crystalline whisker-like Mg2B2O5 crystals.

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